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Journal Article

Reaction of Hydrazine Hydrate with 4-Alkyl-1-Cyanoacetylthiosemicarbazides

C. N. O'Callaghan
Proceedings of the Royal Irish Academy. Section B: Biological, Geological, and Chemical Science
Vol. 76 (1976), pp. 37-41
Published by: Royal Irish Academy
Stable URL: http://www.jstor.org/stable/20519002
Page Count: 5

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Topics: Hydrazines, Ethanol, Hydrates, Salts, Triazoles, Hydroxides, Chemical bases, Sodium, Cyanides
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Since scans are not currently available to screen readers, please contact JSTOR User Support for access. We'll provide a PDF copy for your screen reader.
Reaction of Hydrazine Hydrate with 4-Alkyl-1-Cyanoacetylthiosemicarbazides
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Abstract

4-Alkyl-1-cyanoacetylthiosemicarbazides are cyclised by hydrazine hydrate to 4-alkyl-5-cyanomethyl-1,2,4-triazoline-3-thiones, which at higher temperatures are converted into 4-amino-3,5-di(4-alkyl-3-thioxo-1,2,4-triazolin-5-ylmethyl)triazole derivatives; 4-amino-3,5-di(carbazoylmethyl)-1,2,4-triazole and 4-alkylthiosemicarbazides are also obtained in side-reactions.

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